Dynamic Oxidation Behavior and Exceptional High-Temperature Resistance of Nano Particle-Strengthened Superalloy (MA 754) under Cyclic Temperature Conditions

ABSTRACT: The degradation of industrial components due to high-temperature oxidation poses a significant challenge. This study highlights the excellent oxidation resistance of the MA 754 superalloy under cyclic high-temperature conditions at 1100 °C. The weight change during thermal cycles was measured to assess the kinetics of oxidation. Optical microscopy, scanning electron microscopy, X-ray diffraction, and energy dispersive spectroscopy were used to characterize the oxide scales’ microstructure, morphology, phases, and composition. The results revealed that the MA 754 superalloy demonstrated excellent resistance to oxidation, with a mean net mass change of 0.032 mg/cm² over the oxidation time. The oxidation products identified were NiO and NiCr₂O₄. A small peak suggests the possible formation of Al₂O₃. The oxide scales’ morphology changed from pyramidal to granular type during the oxidation test. The oxidation steps of the MA 754 superalloy were determined by comparing the microstructures of the alloy surface next to the oxide layer.